| HISTORY |
Rosin & Turpentine Factory Nahan is one of the two Rosin Factories under the H.P.
State Forest Corporation. This was established during the year 1949, with M/s Gopal Singh
& Sons as Managing Agents under an agreement drawn during the erstwhile Sirmour
Darbar. From the year 1957-58 to 1958-1959 the overall control of the factory was
transferred to the Industries Deptt. of H.P.and from 1.4.1959 the administrative &
financial control of this factory was handed over to H.P. Forest Deptt. On 1.4.1974 the
management of this factory was handed over to H.P. State Forest Corporation and is
continuing so till date. |

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| PROCESS OF DISTILLATION |
The resin contained in about 400 Tins (7.2
Tons.approx.) is emptied in to the Resin Pit. During winter resin is a bit hard to work,
so 100-200 Litres of Turpentine Oil is mixed to dilute this resin. The Screw Elevator
lifts this resin along with sakki (pine needles, bark pieces & other foreign
particles) to the mixing Vat. The capacity of the Mix Vat is 350-400 tins i.e. about 7.2
Tons. of resin. The resin is heated indirectly in this vat by passing steam through copper
coils for 4 to 6 hours to melt the resin in it. The temperature is maintained upto 950
Celsius. 600-1200 Litres of Turpentine Oil (depending on the quality of resin) is also
mixed in the mixing vat. 5 kgs. Common Salt is added. The molten resin is then stirred
with Iron arms mechanically. The molten resin is then passed through 40-mesh (in one
square inch, there are 40 openings ) stainless steel wire net to remove bigger impurities
like pine needles, bark pieces etc.
From here the resin is pumped by centrifugal pump into a Rest Vat. The capacity of
each rest vat is about 7.2 Tons. The resin is allowed to rest in the rest vat from 18
hours to 20 hours. During this rest period, the impurities and dust if present, settle
down by gravity. The dust/impurities are removed through a bottom valve and sent for
processing separately as inferior grades of Rosin. About 1.7 to 1.8 Tons. of resin from
rest vat is carried to the compression chamber. From compression chamber it is carried to
distillation kettle by steam pressure.
In the
Distillation Kettle, the resin is cooked for 1-2 hours by indirect steam at pressure of
10kgs/cm . In Distillation Kettle, the molten resin remains inside the copper tubes and
steam remains in the outside. In this process the Turpentine Oil and moisture present in
the resin get evaporated and condense in the condenser. T.Oil is collected in a
T.Oil Separator.
The Rosin left in the distillation kettle is taken out at 1650 Celsius &
collected in trolleys ,wherein about 100-200 grams of Oxalic Acid ( depending on the
quality of resin) is mixed to increase the transparency / shine of Rosin. This Rosin is
then packed in Tin Patra Barrels of 200 Kg. capacity.
These items i.e. Rosin and Turpentine Oil are also called Gum Naval Stores in American
markets. This is based on the historical use of rosin for making boats water proof. |

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| ROSIN |
Rosin is a brittle,
faintly aromatic solid, which may be transparent or slightly translucent and possesses a
glassy fracture. It is insoluble in water, but soluble in many organic solvents including
alcohols, ethers and esters, and aliphatic, aromatic and chlorinated hydrocarbons.
Resin acid composition (%) of Pinus roxburghii rosin |
| S.NO |
COMPONENT |
MEAN |
RANGE |
| 1. |
Isopimaric |
20.9 |
19.5 23.1 |
| 2. |
Dihydroabietic |
1.5 |
1.3 2.5 |
| 3. |
Abietic |
37.5 |
35.5 39.4 |
| 4. |
Neoabietic |
15.1 |
14.2 15.8 |
| 5. |
Piamaric |
8.3 |
7.0 - 8.8 |
| 6. |
Levopimaric/palustric |
13.5 |
11.2 15.7 |
All rosin is purchased on a colour basis, which varies from pale amber to black. The
lighter the colour, the more valuable the rosin.
The procedure for sample and colour grading is fairly simple: a portion of rosin is formed
into a cube of 7/8 inch(22mm) sides. This cube is placed inside the cabin of Lovibond
Tintometer and Standard Colour of the specific grade is compared with that of the cube.
The standard colour is obtained by combination
of glass slides of different shades of Red,
Blue and Yellow . This is as per the procedure laid down in IS 553:1984.
Technical specification of various grades of Rosin.
X - Extra
White, WW Water White, WG Window Glass,
NNancy, M Mary, K Kitty, H Harry, D Dark & B
Black.
| USES |
Paper Sizing, printing inks, protective coatings, adhesives, varnishes and
lacquers, grinding and dispersion of pigments, plasticiser & tackifier in rubber and
chewing gums. |
|

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| TURPENTINE
OIL |
Turpentine, like rosin, is a very versatile raw material. At one time turpentine was a
very important solvent and thinner for paint and varnish. In recent years this use has
declined drastically, both on account of substitution by cheaper petroleum-derieved
solvents (white spirits) and because of the growth of paints based upon polymeric latexes.
Whereas in the past turpentine was used mostly in its natural form, today most turpentine
is further processed into its various constituents before use. Since turpentine is mainly
used in its fractionated form, the major fractions of turpentine are given below:
Constituents of turpentine from Pinus
roxburghii |
| S.NO. |
Component |
Mean |
Range |
| 1. |
a- Pinene |
22.8 |
15.6 - 29.7 |
| 2. |
Camphene |
0.4 |
0.3 - 0,.5 |
| 3. |
ß- Pinene |
14.1 |
3.3 - 34.9 |
| 4. |
? 3- Carene |
50.6 |
37.6 - 61.2 |
| 5. |
a- Phellandrene |
0.1 |
0.1 - 0.1 |
| 6. |
a- Terpinene |
0.4 |
0.3 - 0.4 |
| 7. |
Limonene |
0.9 |
0.6 - 1.4 |
| 8. |
ß - Phellandrene |
0.7 |
0.6 - 0.8 |
| 9. |
? - Terpinene |
0.5 |
0.4 - 0.6 |
| 10. |
Terpinolene |
3.2 |
3.0 - 4.6 |
| 11. |
Longipinene |
0.2 |
0.1 - 0.2 |
| 12. |
Longicyclene |
0.2 |
0.1 - 0.2 |
| 13. |
Sativene |
0.1 |
0.1 - 0.1 |
| 14. |
Longifolene |
3.4 |
2.7 - 4.5 |
| 15. |
ß - Caryophyllene |
0.2 |
0.05 - 0.5 |
| 16. |
a- Terpinyl acetate |
0.3 |
0.2 - 0.3 |
Specifications of Turpentine Oil- Grade-II
| Description |
The material is in the form of clear limpid and transparent liquid with a
characteristic odour and pungent and somewhat bitter taste. It is free from sediment,
suspended matter, separated water & added adulterants. |
| S.NO. |
Particulars |
BIS Requirements as per IS: 533-1973 |
Results of T.Oil of R &T Factory, Nahan |
| 1. |
Grease spot test |
Fixed oil absent |
Fixed oil absent |
| 2. |
Relative density at 300 C |
0.852 to 0.868 |
0.854 to 0.868 |
| 3. |
Solubility |
Shall complies |
Complies |
| 4. |
Flash Point |
Not less than 350 C |
380 C to 400 C |
| 5. |
Colour |
Should passes the test |
Passes the test |
| 6. |
Refractive Index at 300 C |
1.468 to 1.475 |
1.468 to 1.473 |
| 7. |
Residue on evaporation |
2.0 % Max. |
1.0 to 1.3 |
| 8. |
Unpolymerizable matter |
11 % Max. |
7 to 9 |
| 9. |
Acid value |
1.5 Max. |
0.5 to 0.7 |
| 10. |
Distillation range
a) at
1550 C
b) up
to 2500 C |
Nil
96 ml Min.
|
Nil
96 ml |
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